As with its predecessor, this edition uses a practical non-mathematical approach. Features a number of recent developments in the field including two-dimensional methods, solid state NMR and an enlarged treatment of Fourier Transform methods. Contains numerous two-color diagrams.
Author: K.V.R. Chary
Publisher: Springer Science & Business Media
Release Date: 2008-04-08
During teaching NMR to students and researchers, we felt the need for a text-book which can cover modern trends in the application of NMR to biological systems. This book covers the entire area of NMR in Biological Sciences (Biomolecules, cells and tissues, animals, plants and drug design). As well as being useful to researchers, this is an excellent book for teaching a course on NMR in Biological Systems.
Author: Ursula Weber
Publisher: John Wiley & Sons
Release Date: 2008-11-21
The state-of-the-art in NMR spectral analysis. This interactive tutorial provides readers with a comprehensive range of software tools and techniques, as well as the necessary theoretical knowledge required to analyze their spectra and obtain the correct NMR parameters. Modern Spectral Analysis provides expert guidance, by presenting efficient strategies to extract NMR parameters from measured spectra. A database of selected spectra and modern, powerful WIN-NMR software designed by Bruker are provided on the enclosed CD-ROM. The programs provided are 1 D WIN-NMR, WIN-DAISY, WIN-DR and WIN-DYNAMICS, and direct data exchange between all these programs is possible. Readers are shown how they can obtain maximum structural information from their 1 D NMR spectra with time-saving computer assistance. Practical problems that can occur and their solutions are discussed at length using clear, easy-to-follow examples. Both homo- and heteronuclear and first- and second-order spin systems are demonstrated. Moreover, relaxation analysis, nuclear Overhauser effects and magnetic site exchange are all covered in this hands-on guide to NMR spectral analysis.
Author: Thomas J. Bruno
Publisher: CRC Press
Release Date: 2010-12-13
Winner of an Oustanding Academic Title Award for 2011! Researchers in organic chemistry, chemical engineering, pharmaceutical science, forensics, and environmental science make routine use of chemical analysis, but the information these researchers need is often scattered in different sources and difficult to access. The CRC Handbook of Basic Tables for Chemical Analysis, Third Edition is a one-stop reference that presents updated data in a handy format specifically designed for use when reaching a decision point in designing an analysis or interpreting results. In response to a decade of reader input, this new edition has been expanded to include even more of the critical information scientists rely on to perform accurate analysis. Enhancements to the Third Edition: Includes data from the CRC Handbook of Fundamental Spectroscopic Correlation Charts into this volume for the first time Presents new information on gas, liquid, and thin layer chromatography; nuclear magnetic resonance spectrometry; infrared spectrophotometry; and mass spectrometry Reviews the detection of outliers in experimental data Provides basic information on thermocouples, chemical indicators, and chromatographic column regeneration Explores the latest stationary phases for chromatographic methods and extractions Examines carcinogens and chemical, electrical, radiation, and laser hazards Includes information on laboratory safety and equipment, from advice on choosing lab gloves and apparel to selecting respirators Unmatched in its coverage of the range of information scientists need in the lab, this resource will be referred to again and again by practitioners who need quick, easy access to the data that forms the basis for experimentation and analysis.
Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicians to study the structure and dynamics of molecules. In recent years, no other technique has grown to such importance as NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR has established itself as a premier means for the specialist and nonspecialist alike to become familiar with new techniques and applications of NMR spectroscopy. Volume 49 continues the tradition with contributions on: novel applications of dynamic NMR in organic chemistry; principles and unconventional aspects of NMR diffusometry; density functional theory and its application to NMR sheilding constants; NMR studies of lac operator lac repressor; and intramolecular interactions of polyethers and polysulphides, investigated by NMR, Ab Initio molecular orbital calculations and the rotational isomeric state scheme. - Includes comprehensive review articles on NMR Spectroscopy - NMR is used in all branches of science - No other technique has grown to such importance as NMR Spectroscopy in recent years
Author: Jan C. J. Bart
Publisher: John Wiley & Sons
Release Date: 2005-04-08
Genre: Technology & Engineering
This industrially relevant resource covers all established and emerging analytical methods for the deformulation of polymeric materials, with emphasis on the non-polymeric components. Each technique is evaluated on its technical and industrial merits. Emphasis is on understanding (principles and characteristics) and industrial applicability. Extensively illustrated throughout with over 200 figures, 400 tables, and 3,000 references.
Daniel Canet hat aus Seminaren und Vorlesungen an der Universität Nancy I die wesentlichen Themen der Kernresonanzspektroskopie ausgewählt. Er stellt die physikalischen Zusammenhänge so dar, daß sich eine große Gruppe für das Buch interessiert: Chemiker, Biochemiker - und auch Mediziner, in deren Diagnostik auch die spektroskopischen Aspekte eine immer größere Rolle spielen. Das Buch ist auf drei Ebenen geschrieben: als Einführung in das physikalische Phänomen, als Lehrbuch für Chemiker nach dem Vordiplom und als eine Darstellung der quantenchemischen Modelle, die zum Verständnis der Spindynamik, der Multipuls- und multidimensionalen Verfahren nötig sind. Hier unterscheidet sich Canets Buch von anderen Einführungen.
Author: Horst Friebolin
Publisher: John Wiley & Sons
Release Date: 2013-02-01
Genre: Nuclear magnetic resonance spectroscopy
Diese vollstandig uberarbeitete und aktualisierte Neuauflage des klassischen Lehrbuches beinhaltet neben den Grundlagen der NMR-Spektroskopie auch die der Spektreninterpretation. Ohne viel Mathematik bietet der Text eine Einleitung und deckt somit auch den Lehrstoff von Hochschulkursen ab. Der Hauptanteil des Buches ist nach wie vor der NMR-Spektroskopie an Losungen gewidmet, doch wurden auch verstarkt Untersuchungen an Festkorpern und die Analyse von Biopolymeren berucksichtigt. Zum Schluss werden einige Einsatzmoglichkeiten der Kernspintomographie und der Kombination von Tomographie und Spektroskopie besprochen. Erganzt wurde jedes Kapitel um Aufgaben, deren Losungsvorschlage im Anschluss an Kapitel 14 zu finden sind. Mit seiner ubersichtlichen Darstellung ist dieses Buch ein Muss fur Studenten, Dozenten und Anwender der NMR-Spektroskopie in der Chemie, Biochemie und Pharmazie.
Spin Resonance Spectroscopy: Principles and Applications presents the principles, recent advancements and applications of nuclear magnetic resonance (NMR) and electron paramagnetic resonance (EPR) in a single multi-disciplinary reference. Spin resonance spectroscopic techniques through NMR and EPR are widely used by chemists, physicists, biologists and medicinal chemists. This book addresses the need for new spin resonance spectroscopy content while also presenting the principles, recent advancements and applications of NMR and EPR simultaneously. Ideal for researchers and students alike, the book provides a single source of NMR and EPR applications using a dynamic, holistic and multi-disciplinary approach. Presents a highly interdisciplinary approach by including NMR and EPR applications in chemistry, physics, biology and biotechnology Addresses both NMR and EPR, making its concepts and applications implementable in multiple resonance environments and core scientific disciplines Features a broad range of methods, examples and illustrations for both NMR and EPR to aid in retention and underscore key concepts
Solving Problems with NMR Spectroscopy, Second Edition, is a fully updated and revised version of the best-selling book. This new edition still clearly presents the basic principles and applications of NMR spectroscopy with only as much math as is necessary. It shows how to solve chemical structures with NMR by giving many new, clear examples for readers to understand and try, with new solutions provided in the text. It also explains new developments and concepts in NMR spectroscopy, including sensitivity problems (hardware and software solutions) and an extension of the multidimensional coverage to 3D NMR. The book also includes a series of applications showing how NMR is used in real life to solve advanced problems beyond simple small-molecule chemical analysis. This new text enables organic chemistry students to choose the most appropriate NMR techniques to solve specific structures. The problems provided by the authors help readers understand the discussion more clearly and the solution and interpretation of spectra help readers become proficient in the application of important, modern 1D, 2D, and 3D NMR techniques to structural studies. Explains and presents the most important NMR techniques used for structural determinations Offers a unique problem-solving approach for readers to understand how to solve structure problems Uses questions and problems, including discussions of their solutions and interpretations, to help readers understand the fundamentals and applications of NMR Avoids use of extensive mathematical formulas and clearly explains how to implement NMR structure analysis Foreword by Nobel Prize winner Richard R. Ernst New to This Edition Key developments in the field of NMR spectroscopy since the First Edition in 1996 New chapter on sensitivity enhancement, a key driver of development in NMR spectroscopy New concepts such as Pulse Field Gradients, shaped pulses, and DOSY (Diffusion Order Spectroscopy) in relevant chapters More emphasis on practical aspects of NMR spectroscopy, such as the use of Shigemi tubes and various types of cryogenic probes Over 100 new problems and questions addressing the key concepts in NMR spectroscopy Improved figures and diagrams More than 180 example problems to solve, with detailed solutions provided at the end of each chapter
89 years of expertise in applied and industrial chemistry - Ullmann's is back in print! Generations of chemists and engineers have relied on the well structured and trusted information from Ullmann's Encyclopedia - and you still can count on Ullmann's with the current 6th edition in print. Ullmann's is a synonym for the world's most current and trustworthy knowledge in everything that relates to the chemical industry, be it processes, chemicals, products, analytical chemistry, pharmaceuticals, biotechnology..........you name it, Ullmann's has it - well over 800 articles on over 30 000 printed pages in 40 volumes. Organized in alphabetical order, the chapters are easy to read and excellent starting points to introduce you to any topic. Over 15 000 tables and 25 000 figures (some of them in color) make it easy for you to quickly find what you are looking for. Countless literature and patent references guide you to the relevant and accessible primary literature. Numerous cross-references point you to relevant chapters in the same context and a well organized index volume enables searching for keywords. Finding what you need is very simple indeed and you won't have to ask for a user's manual for this massive work! Supervised by an internationally acclaimed advisory board, the articles are written by over 3000 international experts from industry and universities, thoroughly edited to uniform style and layout in an in-house office. All figures are re-drawn to give a maximum of clarity and uniformity in style. Compared to the prior edition, almost 60% of the material has either been newly written or thoroughly updated. The rest has been checked for validity and newer references have been added throughout.
Der Band enthält 100 praxisnahe und verständliche Beispiele und Übungen zur korrekten Auswertung von ein- und zweidimensionalen NMR (Nuclear Magnetic Resonance)-Spektren. Alle gängigen Problemstellungen der Spektrenauswertung werden behandelt. Außerdem enthält das Buch eine Liste der wichtigsten Spektrenparameter sowie viele praktische Hinweise. Alle Beispiele und Übungen haben sich in Kursen des Autors bewährt. Sie sind nach verschiedenen Schwierigkeitsgraden ausgewählt und insbesondere auch für das Selbststudium geeignet.
Author: John W. Lehman
Publisher: Pearson College Div
Release Date: 2008-01-25
This comprehensive lab companion provides a thorough introduction to all of the significant operations used in the organic lab, for both traditional-scale and microscale applications. It includes enough theory to help students understand how and why an operation works, but emphasizes the practical aspects of an operation to help them perform the operation successfully in the lab. lab.Makes substantive revisions of many operations to clarify existing material and add new information. Emphasizes environmentally friendly (i.e. green ) lab experiments. Adds a new section on Chemistry and the Environment.A useful guide for chemists and other professionals who do laboratory work in the scientific fields.